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“Decarbonization” of an imino N-heterocyclic carbene ligand via triple benzyl migration from hafnium

19-Mar-2015 | Dipesh Prema; Yohan L. N. Mathota Arachchige; Rex E Murray; LeGrande M. Slaughter, Chemical Communication, 2015

An imino N-heterocyclic carbene underwent three sequential benzyl migrations upon reaction with tetrabenzylhafnium, resulting in complete removal of the carbene carbon from the ligand. The resulting eneamido-amidinato hafnium complex showed alkene polymerization activity comparable to that of a ...

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2-Aryl-3-methyloctahydrophenanthrene-2,3,7-triols as Potent Dissociated Glucocorticoid Receptor Agonists

17-Mar-2015 | Yves A. Chantigny; John C. Murray; Edward F. Kleinman; Ralph P. Robinson; Michael A. Plotkin; Matthew R. Reese; Leon ..., Journal of Medicinal Chemistry, 2015

A significant improvement in agonist activity of the previously described 2-aryloctahydrophenanthrene-2,3,7-triol series of dissociated glucocorticoid receptor agonists (DAGRs) was achieved by modifying the substitution at C3 from (S)-3-hydroxy to (R)-3-hydroxy-3-methyl. The IC50 of the prototype ...

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Inducible and Reversible Lentiviral and Recombination Mediated Cassette Exchange (RMCE) Systems for Controlling Gene Expression

13-Mar-2015 | David C. Bersten et al., PLoS ONE, 2015

by David C. Bersten, Adrienne E. Sullivan, Dian Li, Veronica Bhakti, Stephen J. Bent, Murray L. Whitelaw Manipulation of gene expression to invoke loss of function (LoF) or gain of function (GoF...

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Addition Reactions of Olefins to Asphaltene Model Compounds

10-Mar-2015 | Samuel D. Cardozo; Matthias Schulze; Rik R. Tykwinski; Murray R. Gray, Energy & Fuels, 2015

Addition reactions have been proposed as a significant pathway for coke formation in the liquid-phase cracking of heavy oils and bitumens. In order to study the kinetics of olefin addition in the liquid phase, two alkyl-bridged aromatic compounds, with molecular weights of 899.70 g/mol and ...

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Discovery of a Series of Efficient, Centrally Efficacious BACE1 Inhibitors through Structure-Based Drug Design

09-Mar-2015 | Christopher R. Butler; Michael A. Brodney; Elizabeth M. Beck; Gabriela Barreiro; Charles E. Nolan; Feng Pan; Felix V ..., Journal of Medicinal Chemistry, 2015

The identification of centrally efficacious β-secretase (BACE1) inhibitors for the treatment of Alzheimer’s disease (AD) has historically been thwarted by an inability to maintain alignment of potency, brain availability, and desired absorption, distribution, metabolism, and excretion (ADME) ...

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New Structural Motifs Resulting from Internal Constraints in Chelating Bis(NHC) Ligands: A Dinuclear Ruthenium(II) Complex Featuring an η2-Arene Binding Mode and a Remarkable New Tetrameric Silver(I) Halide Form

09-Mar-2015 | Peter V. Simpson; David H. Brown; Brian W. Skelton; Allan H. White; Murray V. Baker, Organometallics, 2015

A novel dinuclear ruthenium(II) complex containing two ortho-xylylene-linked bis(NHC) ligands (NHC = N-heterocyclic carbene) has been synthesized via transmetalation from a silver-NHC complex. Each ruthenium atom in the dinuclear complex is chelated through the two carbene carbon atoms and, ...

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Large Area Synthesis of a Nanoporous Two-Dimensional Polymer at the Air/Water Interface

04-Mar-2015 | Daniel J. Murray; Dustin D. Patterson; Payam Payamyar; Radha Bhola; Wentao Song; Markus Lackinger; A. Dieter Schlüte ..., Journal of the American Chemical Society, 2015

Journal of the American Chemical Society DOI: 10.1021/ja512018j

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Molecular Characterization of Whey Protein Hydrolysate Fractions with Ferrous Chelating and Enhanced Iron Solubility Capabilities

04-Mar-2015 | Ian B. O’Loughlin; Phil M. Kelly; Brian A. Murray; Richard J. FitzGerald; Andre Brodkorb, Journal of Agricultural and Food Chemistry, 2015

The ferrous (Fe2+) chelating capabilities of WPI hydrolysate fractions produced via cascade membrane filtration were investigated, specifically 1 kDa permeate (P) and 30 kDa retentate (R) fractions. The 1 kDa-P possessed a Fe2+ chelating capability at 1 g L–1 equivalent to 84.4 μM EDTA (for 30 ...

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Simple Preparation of Positively Charged Silver Nanoparticles for Detection of Anions by Surface-Enhanced Raman Spectroscopy

03-Mar-2015 | Steven Bell; Alan Stewart; Shauneen Murray, Analyst, 2015

Modification of citrate and hydroxylamine reduced Ag colloids with thiocholine bromide, a thiol functionalized quaternary ammonium salt, creates particles where the zeta potential is switched from the normal values of ca. -50 mV to ca. +50 mV. These colloids are stable but can be aggregated with ...

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Synthesis, Structure, and Magnetic Properties of Novel B-site Ordered Double Perovskites, SrLaMReO6 (M = Mg, Mn, Co and Ni)

02-Mar-2015 | John E Greedan; Corey M. Thompson; Lisheng Chi; Alannah Hallas; Murray Wilson; Timothy Munsie; Ian Swainson; Andrew ..., Dalton Transactions, 2015

Dalton Trans., 2015, Accepted ManuscriptDOI: 10.1039/C4DT03821E, Paper John E Greedan, Corey M. Thompson, Lisheng Chi, Alannah Hallas, Murray Wilson, Timothy Munsie, Ian Swainson, Andrew Paul...

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