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A (Pentafluoroethyl)(trifluoromethyl)carbene Complex of Iridium and Reductive Activation of its sp3 [small alpha], [small beta] and [gamma] Carbon-Fluorine Bonds to Give Perfluoro-2-butyne, Perfluoro-1,2,3-butatriene and Perfluoro-1-irida-2-methyl-2-cyclobutene) Complexes.

07-Jul-2015 | Jian Yuan; Russ Hughes; Arnold L Rheingold, Dalton Transactions, 2015

The (pentafluoroethyl)(trifluoromethyl)carbene complex Cp*Ir(CO)[=C(CF3)(C2F5)] was synthesized by the reductive activation of the α–C–F bond in the perfluoro-sec-butyl-iridium complex Cp*Ir(CO)[CF(CF3)(C2F5)](I) with Na/Pb alloy. This compound exists as two geometric isomers in solution; the ...

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Direct electrocatalytic and simultaneous determination of purine and pyrimidine DNA bases using novel mesoporous carbon fibers as electrocatalyst

05-Jul-2015 | Author(s): Shuang Ren , Huan Wang , Hongyi Zhang , Liqing Yu , Mingjie Li , Meng Li, Journal of Electroanalytical Chemistry, 2015

Publication date: 1 August 2015 Source:Journal of Electroanalytical Chemistry, Volume 750 Author(s): Shuang Ren , Huan Wang , Hongyi Zhang , Liqing Yu , Mingjie Li , Meng Li Novel mesoporous carbon fibers (MCFs) were fabricated through a self-templating strategy and solution growth ...

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Role of Heavy Meromyosin in Heat‐Induced Gelation in Low Ionic Strength Solution Containing l‐Histidine

04-Jul-2015 | Toru Hayakawa, Yuri Yoshida, Masanori Yasui, Toshiaki Ito, Jun‐ichi Wakamatsu, Akihito Hattori, Takanori Nishimura, Journal of Food Science, 2015

Abstract The gelation of myosin has a very important role in meat products. We have already shown that myosin in low ionic strength solution containing l‐histidine forms a transparent gel after heating. To clarify the mechanism of this unique gelation, we investigated the changes in the nature ...

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Acyclic Pseudopeptidic Hosts as Molecular Receptors and Transporters for Anions

03-Jul-2015 | Inés Martí, M. Isabel Burguete, Philip A. Gale, Santiago V. Luis, European Journal of Organic Chemistry, 2015

Abstract The synthesis and characterization of different pseudopeptidic hosts derived from open chain systems with C2 and C3 symmetry has been achieved. These receptors are based on structures containing phenylalanine amino acid residues and amine, amide, urea and thiourea groups as the ...

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Photoelectrocatalytic oxidation of methyl orange on TiO2 nanotubular anode using a flow‐cell

03-Jul-2015 | María José Martín de Vidales, Laura Mais, Cristina Sáez, Pablo Cañizares, Frank C. Walsh, Manuel A. Rodrigo, Christi ..., Chemical Engineering & Technology, 2015

Abstract Methyl orange from water was removed by photocatalytic anodic oxidation method using a titanium dioxide array surface. The coating was prepared by anodising a titanium plate using NH4F as electrolyte followed by heat treatment to render a photocatalytic surface under UV light. SEM ...

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Structural, Electrical, and Ferroelectric Properties of Nb‐Doped Na0.5Bi4.5Ti4O15 Thin Films

03-Jul-2015 | Chinnambedu Murugesan Raghavan, Jin Won Kim, Sang Su Kim, Journal of the American Ceramic Society, 2015

Ferroelectric Na0.5Bi4.5Ti4O15 (NaBTi) and donor Nb‐doped Na0.5Bi4.5Ti3.94Nb0.06O15 (NaBTiNb) thin films were prepared on Pt(111)/Ti/SiO2/Si(100) substrates using a chemical solution deposition method. The doping with Nb5+‐ions leads to tremendous improvements in the ferroelectric properties of ...

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Alternating Ring-Opening Copolymerization of Cyclohexene Oxide and Maleic Anhydride with Diallyl-Modified Manganese(III)–Salen Catalysts

03-Jul-2015 | Dengfeng Liu, Zhao Zhang, Xingmei Zhang, Xingqiang Lü,, Australian Journal of Chemistry, 2015

Dengfeng Liu, Zhao Zhang, Xingmei Zhang, Xingqiang Lü The ring-opening copolymerization of CHO and maleic anhydride (MA) in bulk and solution was studied in detail using a series of diallyl-modified (salen)Mn complexes. The best catalytic performances were obtained using the following ...

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Nickel Hexacyanoferrate as Suitable Alternative to Ag for Electrochemical Lithium Recovery

02-Jul-2015 | R. Trócoli, A. Battistel, F. La Mantia, ChemSusChem, 2015

Abstract Currently, Li is mainly produced through evaporation of Li‐rich brines obtained from South American countries such as Bolivia, Chile, and Argentina. The most commonly used process, the lime–soda evaporation, requires a long time and several purification steps, which produces a ...

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Effects of Mg17Sr2 Phase on the Bio‐Corrosion Behavior of Mg–Zr–Sr Alloys

02-Jul-2015 | Yunfei Ding, Yuncang Li, Cuie Wen, Advanced Engineering Materials, 2015

The effect of the second phase Mg17Sr2 on the biocorrosion behavior of Mg5ZrxSr (x = 0, 2, 5 wt%) alloys before and after solution treatment was investigated. Electrochemical impedance spectroscopy, cathodic polarization and hydrogen evolution were used to evaluate the biocorrosion of Mg5ZrxSr. ...

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ChemInform Abstract: Stark Sublevels in Tm3+—Yb3+ Codoped Na2Y2B2O7 Nanophosphor for Multifunctional Applications.

02-Jul-2015 | Abhishek Kumar Soni, Riya Dey, Vineet Kumar Rai, ChemInform, 2015

Abstract Tm3+, Yb3+ co‐doped Na2Y2B2O7 with an average crystallite size of 18‐20 nm is prepared by solution combustion of a stoichiometric mixture of Y2O3, H3BO3, Na2CO3, Tm2O3, and Yb2O3 in conc.

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