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Rhodium(III) cationic methyl complexes containing dimethylformamide ligand, cis-[Rh(β-diket)(PPh3)2(CH3)(DMF)][BPh4] (β-diket = acetylacetonate or benzoylacetonate), in comparison with their acetonitrile analogs

17-10-2014 | Author(s): Elizaveta P. Shestakova , Yuri S. Varshavsky , Victor N. Khrustalev , Galina L. Starova , Sergei N. ..., Journal of Organometallic Chemistry, 2014

Publication date: 15 December 2014 Source:Journal of Organometallic Chemistry, Volume 774 Author(s): Elizaveta P. Shestakova , Yuri S. Varshavsky , Victor N. Khrustalev , Galina L. Starova , Sergei N. Smirnov The rhodium(III) cationic methyl complexes, ...

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Phosphorescent Polymeric Nanoparticles by Coordination Cross‐Linking as a Platform for Luminescence Imaging and Photodynamic Therapy

16-10-2014 | Yang Lu, Fengfeng Xue, Zhiguo Zhou, Min Shi, Yuping Yan, Lijie Qin, Hong Yang, Shiping Yang, Chemistry - A European Journal, 2014

Abstract Water‐soluble phosphorescent polymeric nanoparticles with an average diameter of approximately 100 nm were synthesized by a coordination cross‐linking reaction. The pyridine blocks in poly(4‐vinyl pyridine‐b‐ethylene oxide) (P4VP‐b‐PEO) were cross‐linked by the iridium ...

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Alkali metal salts of formazanate ligands: diverse coordination modes as a result of the nitrogen-rich [NNCNN] ligand backbone

15-10-2014 | Edwin Otten; Raquel Travieso-Puente; Mu-Chieh Chang, Dalton Transactions, 2014

Alkali metal salts of redox-active formazanate ligands were prepared, and their structures in the solid-state and solution determined. The nitrogen-rich [NNCNN] backbone of formazanates results in a varied coordination chemistry, with both the internal and terminal nitrogen atoms available for ...

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A new three‐dimensional anionic cadmium(II) dicyanamide network

14-10-2014 | Qiang Li, Hui‐Ting Wang, Acta Crystallographica Section C, 2014

A new cadmium dicyanamide complex, poly[tetramethylphosphonium [μ‐chlorido‐di‐μ‐dicyanamido‐κ4N1:N5‐cadmium(II)]], [(CH3)4P][Cd(NCNCN)2Cl], was synthesized by the reaction of tetramethylphosphonium chloride, cadmium nitrate tetrahydrate and sodium dicyanamide in aqueous solution. In the crystal ...

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Dilithium Hexaorganostannate(IV) Compounds

14-10-2014 | Ireen Schrader, Kornelia Zeckert, Stefan Zahn, Angewandte Chemie International Edition, 2014

Abstract Hypercoordination of main‐group elements such as the heavier Group 14 elements (silicon, germanium, tin, and lead) usually requires strong electron‐withdrawing ligands and/or donating groups. Herein, we present the synthesis and characterization of two hexaaryltin(IV) dianions in form ...

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Active layer solution-processed NIR-OLEDs based on ternary erbium(III) complexes with 1,1,1-trifluoro-2,4-pentanedione and different N,N-donors

14-10-2014 | Pablo Martin-Ramos; Carmen Coya; Victor Lavín-della-Ventura; Inocencio Rafael Martín-Benenzuela; Manuela Ramos Silva ..., Dalton Transactions, 2014

Using a fluorinated 1,1,1-trifluoro-2,4-pentanedione (Htfac) ligand and either 2,2’-bipyridine (bipy), bathophenanthroline (bath) or 5-nitro-1,10-phenanthroline (5NO2phen) as ancillary ligands, three new ternary erbium(III) octacoordinated complexes have been synthetized. The single crystal ...

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Syntheses, characterization, and electrochemistry of compounds containing 1-diphenylphosphino-1′-(di-tert-butylphosphino)ferrocene (dppdtbpf)

13-10-2014 | Author(s): Manoj Trivedi , Sanjeev Kumar Ujjain , Gurmeet Singh , Abhinav Kumar , Santosh Kumar Dubey , Nigam P ..., Journal of Organometallic Chemistry, 2014

Publication date: 1 December 2014 Source:Journal of Organometallic Chemistry, Volumes 772–773 Author(s): Manoj Trivedi , Sanjeev Kumar Ujjain , Gurmeet Singh , Abhinav Kumar , Santosh Kumar Dubey , Nigam P. Rath The reaction of copper(I) salts CuX (X=Cl, Br, I, CN, SCN), ...

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Bioactivity of pyridine-2-thiolato-1-oxide metal complexes: Bi(III), Fe(III) and Ga(III) complexes as potent anti-Mycobacterium tuberculosis prospective agents

12-10-2014 | Author(s): Ignacio Machado , Leonardo Biancolino Marino , Bruno Demoro , Gustavo A. Echeverría , Oscar E. Piro ..., European Journal of Medicinal Chemistry, 2014

Publication date: 24 November 2014 Source:European Journal of Medicinal Chemistry, Volume 87 Author(s): Ignacio Machado , Leonardo Biancolino Marino , Bruno Demoro , Gustavo A. Echeverría , Oscar E. Piro , Clarice Q.F. Leite , Fernando R. Pavan , Dinorah Gambino In the search for ...

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The relevance of ligand exchange kinetics in the measurement of iron speciation by CLE–AdCSV in seawater

12-10-2014 | Author(s): Luis M. Laglera , Montserrat Filella, Marine Chemistry, 2014

Publication date: Available online 28 September 2014 Source:Marine Chemistry Author(s): Luis M. Laglera , Montserrat Filella CLE–AdCSV (competitive ligand exchange–adsorptive cathodic stripping voltammetry) has proved to be a decisive technique in recognising the key role that organic ...

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Iridium Complexes Containing Mesoionic C Donors: Selective C(sp3)H versus C(sp2)H Bond Activation, Reactivity Towards Acids and Bases, and Catalytic Oxidation of Silanes and Water

10-10-2014 | Ana Petronilho, James A. Woods, Helge Mueller‐Bunz, Stefan Bernhard, Martin Albrecht, Chemistry - A European Journal, 2014

Abstract Metalation of a C2‐methylated pyridylimidazolium salt with [IrCp*Cl2]2 affords either an ylidic complex, resulting from C(sp3)H bond activation of the C2‐bound CH3 group if the metalation is performed in the presence of a base, such as AgO2 or Na2CO3, or a mesoionic complex via ...

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