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Warming up for mechanosynthesis - Temperature development in ball mills during synthesis

We present a first direct measurement of the temperature during milling combined with in situ Raman spectroscopy monitoring. The data reveal a low temperature increase due to the mechanical impact and clear temperature increases as a consequence of the reaction heat. Based on the data, temperature rises as p

Authors:   Hannes Kulla; Manuel Wilke; Franziska Fischer; Mathias Röllig; Christiane Maierhofer; Franziska Emmerling
Journal:   Chemical Communication
DOI:   10.1039/C6CC08950J
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