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Sonogashira Coupling in 3D-Printed NMR Cuvettes: Synthesis and Properties of Arylnaphthylalkynes

3D-Printing has been used to build hollow NMR tube/spinner combinations out of NMR-transparent polyamide. The whole 3D-print has been processed inside a glove box and during pauses of the 3D-printing process, all reactants for the palladium-catalyzed decarboxylative Sonogashira coupling of aryl halides with

Authors:   Felix Lederle; Frederick Meyer; Christian Kaldun; Jan C. Namyslo; Eike G. Hübner
Journal:   New Journal of Chemistry
DOI:   10.1039/C6NJ03614G
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