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Molbank, Vol. 2018, Article M995: 2,4-Bis[(2,6-diisopropylphenyl)imino]-3-methylpentan-3-ol

Molbank, Vol. 2018, Article M995: 2,4-Bis[(2,6-diisopropylphenyl)imino]-3-methylpentan-3-ol

Molbank doi: 10.3390/M995

Authors: Wenting Sun Wenyu Kong Qing Du Shumiao Zhang Lihua Guo Zhe Liu

The compound 2,4-bis[(2,6-diisopropylphenyl)imino]-3-methylpentan-3-ol was synthesized with a yield of approximately 80% by the reaction of 2,4-bis(2,6-diisopropylphenylimino)pentan-3-one with trimethylaluminum, which was followed by hydrolysis with an aqueous NaOH solution. A chemoselective addition to the C=O bond occurred in this reaction. The structure was confirmed by X-ray crystallography. This new compound was also fully characterized by 1H, 13C-NMR spectroscopy and 1H-13C HSQC spectroscopy, mass spectrometry and elemental analysis.

Authors:   Sun, Wenting ; Kong, Wenyu ; Du, Qing ; Zhang, Shumiao ; Guo, Lihua ; Liu, Zhe
Journal:   Molbank
Volume:   2018
edition:   2
Year:   2018
Pages:   M995
DOI:   10.3390/M995
Publication date:   12-May-2018
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