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Molbank, Vol. 2018, Article M988: Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine
Molbank doi: 10.3390/M988
Authors: Alessandra Casnati Elena Motti Nicola Ca’
The title compound—cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine—was synthesized in 83% isolated yield by a palladium-catalyzed one-pot strategy from 1-iodo-2-isopropoxybenzene and ortho-bromoaniline. The azepine derivative was fully characterized (FT-IR, MS, 1H and 13C-NMR, elemental analysis) and all proton and carbon signals have been completely assigned by 2D NMR experiments.
| Authors: | Casnati, Alessandra ; Motti, Elena ; Ca’, Nicola Della | |
| Journal: | Molbank | |
| Volume: | 2018 | |
| edition: | 1 | |
| Year: | 2018 | |
| Pages: | M988 | |
| DOI: | 10.3390/M988 | |
| Publication date: | 12-Mar-2018 |
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