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Molbank, Vol. 2018, Article M988: Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine

Molbank, Vol. 2018, Article M988: Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine

Molbank doi: 10.3390/M988

Authors: Alessandra Casnati Elena Motti Nicola Ca’

The title compound—cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine—was synthesized in 83% isolated yield by a palladium-catalyzed one-pot strategy from 1-iodo-2-isopropoxybenzene and ortho-bromoaniline. The azepine derivative was fully characterized (FT-IR, MS, 1H and 13C-NMR, elemental analysis) and all proton and carbon signals have been completely assigned by 2D NMR experiments.

Authors:   Casnati, Alessandra ; Motti, Elena ; Ca’, Nicola Della
Journal:   Molbank
Volume:   2018
edition:   1
Year:   2018
Pages:   M988
DOI:   10.3390/M988
Publication date:   12-Mar-2018
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