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Incorporation of Sb5+ into CeO2: Local Structural Distortion of the Fluorite Structure From a Pentavalent Substituent

Hydrothermal crystallisation of CeO2 from aqueous sodium hydroxide solution at 240 ○C using CeCl3·7H2O in the presence of hydrogen peroxide with addition of either SbCl3 or SbCl5 yields polycrystalline samples of antimony-containing ceria directly from solution. Powder X-ray diffraction shows a contraction o

Authors:   Craig Hiley; Janet Fisher; Reza Jalili Kashtiban; Giannantonio Cibin; David Thompsett; Richard I Walton
Journal:   Dalton Transactions
DOI:   10.1039/C8DT01750F
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