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Development and applications of a sample controlled DSC system

The development of a new sample controlled thermal analysis technique based on a heat flux DSC is described. The performance of the system is demonstrated by studies on the decomposition of sodium bicarbonate and the oxidation of a copper impregnated carbon. The ability of the technique to study reactions which take place without a change in mass is illustrated by the curing of an epoxy resin with a polyaminoamide hardener.

Authors:   E. L. Charsley, P. G. Laye, G. M. B. Parkes, J. J. Rooney
Journal:   Journal of Thermal Analysis and Calorimetry
Year:   2010
DOI:   10.1007/s10973-010-1196-8
Publication date:   20-Dec-2010
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