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Dizincation of a 2‐Substituted Thiophene: Constructing a Cage with a [16]Crown‐4 Zincocyclic Core

Metal detector: A bowl‐shaped nanomolecule (see picture; S yellow, C gray, Zn blue) containing an unprecedented 16‐atom [ZnC3]4 “anti‐crown” ring has been unearthed by isolating a dizincated 2‐substituted thiophene intermediate that would normally be hidden in tandem functionalization methodology.

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Authors:   Liam Balloch, Jennifer A. Garden, Alan R. Kennedy, Robert E. Mulvey, Toni Rantanen, Stuart D. Robertson, Victor Snieckus
Journal:   Angewandte Chemie International Edition
Year:   2012
Pages:   n/a
DOI:   10.1002/anie.201203344
Publication date:   08-Jun-2012
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