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Characterization of Dispersion Effects on Reaction Optimization and Scale-Up for a Packed Bed Flow Hydrogenation Reactor

John W. Eschelbach, David Wernick, Marian C. Bryan, Elizabeth M. Doherty

We analyzed the dispersion for a commercial H-Cube® hydrogenation flow chemistry platform and the effects of dispersion on low volume reactions. Attempts to scale reactions <2 mL were shown to be unreliable. Using larger volumes or replicate small injections proved to be a more consistent approach.


Authors:   John W. Eschelbach, David Wernick, Marian C. Bryan, Elizabeth M. Doherty,
Journal:   Australian Journal of Chemistry
Year:   2012
DOI:   10.1071/CH12450
Publication date:   17-Dec-2012
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