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212 Newest Publications about the topic method validation

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Validated UPLC-MS/MS method for the quantification of dasatinib in plasma: Application to pharmacokinetic interaction studies with nutraceuticals in Wistar rats

14-Jun-2018 | Hadir M. Maher; Nourah Z. Alzoman; Shereen M. Shehata; Norah O. Abanmy, PLoS ONE, 2018

by Hadir M. Maher, Nourah Z. Alzoman, Shereen M. Shehata, Norah O. Abanmy Dasatinib (DAS) is a tyrosine kinase inhibitor (TKI) used in the treatment of chronic myeloid leukemia and in the management of ulcerative colitis (UC). Since some nutraceuticals (e.g. curcumin, olive oil, and cocoa ...

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Molecules, Vol. 23, Pages 884: Application of High-Performance Liquid Chromatography Coupled with Linear Ion Trap Quadrupole Orbitrap Mass Spectrometry for Qualitative and Quantitative Assessment of Shejin-Liyan Granule Supplements

11-Apr-2018 | Gu, Jifeng ; Wu, Weijun ; Huang, Mengwei ; Long, Fen ; Liu, Xinhua ; Zhu, Yizhun, Molecules, 2018

Molecules, Vol. 23, Pages 884: Application of High-Performance Liquid Chromatography Coupled with Linear Ion Trap Quadrupole Orbitrap Mass Spectrometry for Qualitative and Quantitative Assessment of Shejin-Liyan Granule Supplements Molecules doi: 10.3390/molecules23040884 Authors: Jifeng ...

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Molecules, Vol. 23, Pages 173: Pharmacokinetics of Schizandrin and Its Pharmaceutical Products Assessed Using a Validated LC–MS/MS Method

15-Jan-2018 | Li, Chi-Lin ; Cheng, Yung-Yi ; Hsieh, Chen-Hsi ; Tsai, Tung-Hu, Molecules, 2018

Molecules, Vol. 23, Pages 173: Pharmacokinetics of Schizandrin and Its Pharmaceutical Products Assessed Using a Validated LC–MS/MS Method Molecules doi: 10.3390/molecules23010173 Authors: Chi-Lin Li Yung-Yi Cheng Chen-Hsi Hsieh Tung-Hu Tsai Schisandra chinensis has been used ...

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Development and Validation of an Assay to Analyze Atazanavir in Human Hair Via Liquid Chromatography‐Tandem Mass Spectrometry (LC‐MS/MS)

09-Jan-2018 | Nhi Phung, Karen Kuncze, Hideaki Okochi, Alexander Louie, Leslie Z. Benet, Igho Ofokotun, David W. Haas, Judith S. C ..., Rapid Communications in Mass Spectrometry, 2018

Abstract Assays to quantify antiretrovirals in hair samples are increasingly used to monitor adherence and exposure in both HIV prevention and treatment studies. Atazanavir (ATV) is a protease inhibitor used in combination antiretroviral therapy (ART). We developed and validated a liquid ...

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Molecules, Vol. 22, Pages 1853: Simultaneous Determination of Twenty-Five Compounds in Rat Plasma Using Ultra-High Performance Liquid Chromatography-Polarity Switching Tandem Mass Spectrometry and Its Application to a Pharmacokinetic Study

30-Oct-2017 | Zhang, Na ; Li, Yueting ; Sun, Jing ; Li, Chun ; Song, Yuelin ; Li, Jun ; Tu, Pengfei ; Zhao, Yunfang, Molecules, 2017

Molecules, Vol. 22, Pages 1853: Simultaneous Determination of Twenty-Five Compounds in Rat Plasma Using Ultra-High Performance Liquid Chromatography-Polarity Switching Tandem Mass Spectrometry and Its Application to a Pharmacokinetic Study Molecules doi: ...

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Interlaboratory Reproducibility of Droplet Digital Polymerase Chain Reaction Using a New DNA Reference Material Format

18-Oct-2017 | Leonardo B. Pinheiro; Helen O’Brien; Julian Druce; Hongdo Do; Pippa Kay; Marissa Daniels; Jingjing You; Daniel Burke ..., Analytical Chemistry, 2017

Use of droplet digital PCR technology (ddPCR) is expanding rapidly in the diversity of applications and number of users around the world. Access to relatively simple and affordable commercial ddPCR technology has attracted wide interest in use of this technology as a molecular diagnostic tool. ...

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Determination of trace levels of ammonia in marine waters using a simple environmentally-friendly ammonia (SEA) analyser

14-Oct-2017 | Author(s): Lenka O'Connor Šraj, M. Inês G.S. Almeida, Ian D. McKelvie, Spas D. Kolev, Marine Chemistry, 2017

Publication date: 20 August 2017 Source:Marine Chemistry, Volume 194 Author(s): Lenka O'Connor Šraj, M. Inês G.S. Almeida, Ian D. McKelvie, Spas D. Kolev A simple environmentally-friendly ammonia (SEA) analyser based on programmable flow was developed for the determination of trace ...

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Single standard substance for the determination of nine volatile components in the distillate of Fructus Gardeniae and Radix Curcumae (an intermediate of Xingnaojing Injection)

31-Aug-2017 | Jinyang Fang, Bo Yang, Zhiwei Ge, Xue Bai, Binjun Yan, Journal of Separation Science, 2017

Xingnaojing Injection is a traditional Chinese medicine extensively used for stroke and cerebral ischemia. For better in‐process quality control of Xingnaojing Injection, a method for the analysis of its intermediate (i.e., the distillate of Fructus Gardeniae and Radix Curcumae) is needed to ...

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Stereoselective determination of dufulin in watermelon under field conditions using chiral ultra high performance liquid chromatography with high‐resolution mass spectrometry

26-Aug-2017 | Kunming Zheng, Jin Gong, Xiaoqin Li, Guifei Jia, Sizhuo Wu, Haizhen Zhang, Deyu Hu, Kankan Zhang, Journal of Separation Science, 2017

An effective and sensitive chiral analytical method was established to investigate the stereoselective dissipation of rac‐dufulin in watermelon using ultra‐high‐performance liquid chromatography with a Superchiral S‐OD chiral column (4.6mm × 150mm i.d., 5 μm) coupled with high‐resolution mass ...

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Quantitative Analysis of Ingenol in Euphorbia species via Validated Isotope Dilution Ultra‐high Performance Liquid Chromatography Tandem Mass Spectrometry

08-Aug-2017 | Tibor Béres, Klaus Dragull, Jiří Pospíšil, Danuše Tarkowská, Martin Dančák, Ondřej Bíba, Petr Tarkowski, Karel Dolež ..., Phytochemical Analysis, 2017

Abstract Introduction Various species of the Euphorbia genus contain diterpene ingenol and ingenol mebutate (ingenol‐3‐angelate), a substance found in the sap of the plant Euphorbia peplus and an inducer of cell death. A gel formulation of the drug has been approved by the US Food and Drug ...

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