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27 Newest Publications about the topic thermal analyzers


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Reduction Kinetics of Cu-Based Oxygen Carriers for Chemical Looping Air Separation

14-Aug-2013 | Kun Wang; Qingbo Yu; Qin Qin, Energy & Fuels, 2013

The knowledge of the kinetics of oxygen carriers is essential for the design of chemical looping air separation (CLAS) system. In this paper, the Cu-based oxygen carriers were prepared via a mechanical mixing method, and ZrO2, TiO2, and SiO2 were used as binder. The kinetics of the oxygen ...


Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction

08-Apr-2013 | Materials Chemistry and Physics, 2013

15 May 2013 Publication year: 2013Source:Materials Chemistry and Physics, Volume 139, Issues 2–3 The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O87 nanopowders. Phase formation of zinc niobate was ...


Study on inclusion interaction of hydrophilic 2-chloromandelic acid with hydroxypropyl-β-cyclodextrin

27-Nov-2012 | Ping Xu, Xinyu Jiang, Congshan Zhou, Kewen Tang, Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2012

The inclusion interaction between hydroxypropyl-β-cyclodextrin (HP-β-CD) and hydrophilic 2-chloromandelic acid (CMA) was studied by ultraviolet (UV) absorption spectrophotometer. A reliable determination of the complex stoichiometry was provided by the continuous variation technique. 1H NMR ...


Application of a Simultaneous TGA-DSC Thermal Analysis System for High-Throughput Screening of Catalytic Activity

01-Nov-2012 | Jonas Loskyll; Wilhelm F. Maier; Klaus Stoewe, Journal of Combinatorial Chemistry, 2012

We present here the use of a simultaneous TGA/DSC thermal analyzer as a high-throughput reactor system to measure after calibration the heat of reaction and therefore the catalytic activity of heterogeneous catalysts in a fast, reliable and reproducible manner. By coupling the gas outlet of the ...


Membranes of poly(phenylene oxide) and its copolymers: Synthesis, characterization, and application in recovery of propylene from a refinery off‐gas mixture

16-May-2012 | Gajbhiye, Susheela Bai, Journal of Applied Polymer Science, 2012

Abstract Copolymers of 2,6‐dimethyl‐phenol (DMP) and 2,6‐diphenyl‐phenol (DPP) were synthesized in the initial molar ratio of 100 : 0 (S(PPO)), 90 : 10 (Co‐A), 75 : 25 (Co‐B), 65 : 35 (Co‐C), and 0 : 100 (PDPPO). Dense membranes of 30 μm thickness were tested for single gas permeation and ...


Physical and thermal mechanical properties of corn starch/LDPE composites

15-May-2012 | Oromiehie, A. R.; lari, T. Taherzadeh; Rabiee, A., Journal of Applied Polymer Science, 2012

Abstract The potential of biodegradable polymers has long been recognized. In this work, composites of low density polyethylene (LDPE) and low density polyethylene/thermoplastic starch (LDPE/TPS) at different ratios of TPS (40%‐60% w/w) were prepared in internal mixer. Polyethylene‐grafted ...


Effect of Bimetallic Soybean Oil Based Polymer on Growth and Plasma Membrane H+-ATPase Activity Among Fungi

23-Apr-2012 | Taruna Singh, Sumbul Ambreen, Sheikh Shreaz, Athar Adil Hashmi, Journal of Polymers and the Environment, 2012

In view of bio-inorganic importance, iron and zinc incorporated soybean oil based polymer was prepared by condensation polymerization of oil based fatty amide polyole, sebacic acid, zinc acetate and ferric chloride in a process initiated by sodium ethoxide. Microwave assisted synthesis was used ...


Comparative Study of the Effect of Different Coal Fly Ashes on the Performance of Oxygen Carriers for Chemical Looping Combustion

27-Jan-2012 | Aurora Rubel; Yi Zhang; James K. Neathery; Kunlei Liu, Energy & Fuels, 2012

The application of chemical looping combustion (CLC) to solid fuels for the purpose of electric power generation from coal is the focus of research at the Center for Applied Energy Research (CAER), University of Kentucky, Lexington, KY. One important aspect for the use of CLC for solid fuels is ...


Preparation of Cadmium(II) Oxide Nanoparticles from a New One-Dimensional Cadmium(II) Coordination Polymer Precursor; Spectroscopic and Thermal Analysis Studies

24-Jan-2012 | Mahmood Payehghadr, Vahid Safarifard, Maryam Ramazani, Ali Morsali, Journal of Inorganic and Organometallic Polymers and Materials, 2012

A one-dimensional Cd(II) coordination polymer containing 2-pyridinecarboxylate (2-pyc−) and iodide anions [Cd(μ-2-pyc)(μ-I)]n (1), is synthesized and characterized by elemental analysis, IR spectroscopy, thermal analysis and X-ray crystallography. The single-crystal X-ray data show that the ...


Effect of Water Vapor on the Redox Reactions of Iron-Based Oxygen Carriers for Chemical Looping Combustion

20-Sep-2011 | Aurora M. Rubel; Yi Zhang; James K. Neathery; Kunlei Liu, Energy & Fuels, 2011

Iron-based oxygen carriers (OCs) have been the focus of studies at the Center for Applied Energy Research (CAER), University of Kentucky, for the application of chemical looping combustion (CLC) to solid fuels. Freeze granulation (FG) was chosen as a method to produce Fe2O3 on an alumina (Al2O3) ...


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